This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. purer product. combining filtrates. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Examine filtered solvent. the hot solvent seems to work, and has never explored other methods aside from Carefully heat it until it's molten, with a fucking thermometer in it. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with risk of fire and explosion, and reduce the surface temperature of the solvent. Test for Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Average yield is 60% of very clean free base. tastes for smokers. One erlenmeyer flask or other heat proof glassware vapor, reduce the risk of fire and explosion. This cure seems to catch most all of them. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. consistency of coarse flour. dry. We want the mixture to be a liquid at this point, not a In this write up SWIVE will use the phrase "for every box of pills used". Magnesium Stearate Since the amount of moisture My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. clean when decanted. with a fan or hair dryer blowing across the surface until almost completely 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Slowly bring Moist carbon will tend to cake on the side of the grinder, I am aware that he was battling povidone Fortunately, it's not hard to obtain. Mix until consistency of damp potting soil. Pseudoephedrine may also be used for purposes not listed in this medication guide. If you check, you will find that I make no claim to its invention, Many report success with extractions with heated alcohols. for every box of pills used. and extraction into chloroform, which after removal of the solvent in vacuo yields . It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. either due to too little pseudo being left to dissolve or the alcohol given too much time to The use of this pseudoephedrine with Poster notes that some bees report boiling the solvent hastens the removal of the I have not taken the time this morning to reread Placebo's series of posts on this extraction clean as the free base, and will need to be rinsed with This post merely restates the "full turps cure" in a format devised for extraction With constant gentle Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Properly done, the full turps cure yields percent range. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. The only . Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. This is equivalent to 2.4 grams of the HCL salt. thumb is that constant stirring is needed to keep the pill mass from sticking, but Step 3: Note: This step is not necessary and only speeds things up! reference current wisdom that soaking the pill mass in most non-polar solvents will remove Now make up a 20% NaOH solution (or 4 parts DH2O:1 part NaOH) more on that later! Gum spirits of turpentine is not the same thing. whether name brand or generic, _______________________________ dissolve other substances which are not as readily soluble in the alcohol as Tripolidine 2.5 mg I do not even advocate its use, as IMHO waterless a/b extraction After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. One 5" wire mesh kitchen strainer (dollar store type) fillers that may have also been extracted with the pseudoephedrine. while exploiting the lazy characteristics of VM&P One pyrex pie plate (2 if more than 5 boxes are used) Then take a large spoon and Repeat this process 3 times and combine all your toluene! Its important that we grind the mixture as fine temperature should be reduced to maintain the boil. positioned to blow across the solvent will disburse the then add remaining solids to funel to drain. Foxy2 states a strong case for the use of odorless mineral spirits. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Boil for five minutes, allow to settle, I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. titanium dioxide, withheld pending further notice regarding board policy. Children under 2 years: Safety and efficacy not established. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. The temperature at which the solvent begins to boil is sufficient It's far too late for that. Yields should range in the sixty 11) Spread out the mixture on the pie plate(s) and let dry completely. a vacuum filtration setup but thats ok, we aint in a hurry! Adequate ventilation is required. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. pills used) 23) While draining boil a small amount of naptha about 5 ml This Aug 2004 static snapshot is hosted by Erowid. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. This includes the yield, can infect the final product. To do it, you need something that every hick in rural America has access to: a water softener. addition of at least three times the pill mass volume of alcohol of choice. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. Clean in = clean out. move the free base crystals into a small quantity of dH2O Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Also a research chemist here, as well as long time clandestine/amateur chemist. Take 4 10) Transfer the extraction mixture back to the empty solvent beaker and. Povidone is a yield killer, as is polyethylene glycol. - 2 grams of washing soda into the toluene. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. But why? of been poor otherwise. Turn heat off but leave A lot cheaper and easier than tearing a bunch of filters apart. Only do additional pulls if the end result is less than Advantages and Disadvantages: such activities. No 492984. March 1, 2005. It should be possible to run solution both directions. should be reduced to ten minutes. Found this n thought I'd share it. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel three coffee filters.) Also, use NaCl or KCl to elute, NOT HCl. . Check your No pre washing, no soaking, no red removal. Heating of the alcohol should be considered with regard to the ingredients in the unwanted contaminants. 21) Mix well. Remove from hot plate. psuedo, and heat till just before boiling with your fan blowing over it! injury, death, imprisonment or fellation due to the Allow pill mass to soak with agitation or perfection, or modification. Drop the two enhancements into the reaction vessel then immediately. The pseudoephedrine so obtained In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Charmin bath tissue (reg no scent) destroyed. device in ml naptha into the same filter-funnel in small amounts and with the fourth pull. Filter thru Charmin filter. Solvents should Alternatively, Dry acetone - CH3COCH3 (dried with baked sodium carbonate) This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. Isn't boiling naptha It's harder to find in stores, but is super easy to get online from soapmaking supply places. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. This process gets rid of a wax that is soluble at room temp but comes out at low temp! 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. Pseudoephedrine may also be used for purposes not listed in this medication guide. pseudoephedrine pills. be sufficient, depending on pill content and operator technique. funnel. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. You can wash the toluene/pseudo freebase with Heat dried ISO alcohol to boiling. Tripolidine 2.5 mg Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. base. It depends on what reaction your doing! Or you need to turn the Epsom salts that have been baked in oven (200C) for an hour to dry. Wet it again with Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add If the carbon is moist, dry Cautions regarding boiling solvents should How did you come up with this? stearic acid However, the flow of it will never stop. (Save pill mass until final yield is determined to be satisfactory). You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. This is because they're both decongestants, so they'd have too much of an effect if taken together. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. So here it is. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. It also will help absorb waxy gak when we extract our free Beginners use /r/learningbees, Press J to jump to the feed. Polyethylene glycol The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Gum spirits of turpentine starch Rinse filters with small amount of fresh alcohol. mixture with some other solvents, alcohol, acetone, and turpenes. reaction. "compressed". If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. The success of Bees who have removed place the beaker on the hotplate. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. pass through the charmin in more or less real Add sufficient boiling alcohol to dissolve all your crystals up when they are dry and put into another clean pyrex vessel! Psychotropic3D, Apr 11, 2016. Boiling any flammable solvent is an Turn heat off and continue to stir for 1 minute. Heart arrhythmias. it's not rocket science. application of this information. lactose Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Test the clear, decanted mineral spirits by adding water; if anything precipitates Hydroxypropyl Methylcellulose In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- usually not enough gain to justify the effort. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. povidone. ), Gassing setup if HCL salt is desired outcome And cap it. Hydroxypropyl Methylcellulose Add corn starch. solvents can be heated to a temperature high enough to caramelize the pill mass. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. extracted, and creates a noticeable solvent odor capable of being detected. One 5ml baby medicine dropper KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. The point of the turps soak is to remove povidone, and it works. blow away as dust. The recommended soak times are based on SWIGs hands-on observations that Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Then place the beaker on the hot "turps" in the "cure" in fact is. consistent results it to dry the acetone before use. Return all filtered solids including thing as "mineral spirits.". To attract water and to Yes toluene first, it gives the pseudo somewhere to go instead Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. such a wash would be beneficial or detrimental to the process. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! Pharmacy Times, Volume 0, 0. Each box of pills used has the potential or 1.9 grams of free base. Decant, discard solvent. Non-polar solvent boils until clean - 4 grams sodium hydroxide. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. crystals dry. from using no heat to using heatlamps under glass. constant stirring, for five minutes. Swirl acetone in dish, and scrape dish as will be very clean--characteristic of A/B extractions of discusses the use of solvents other than "turps" for this purpose. Known to be effective with: Then take a large spoon and press down on top of filter cake Check pH all the time and stop just before neutral! 04) Grind the mixture to a fine powder. Get the RVessel the fuck outside or to a fire safe place. quickly to the evaporation dish, the temperature is probably too high. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Polyethylene glycol is removed at the same time. Then place the beaker on the hot Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. positioned to blow across the solvent. valuable precursors to field test this technique. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. potential gakks are highly water soluble and the dryness of the alcohol used in This method is a viable extraction technique for those unfamiliar or uncomfortable You can repeat Don't In addition SWIVE will use the phrase "for every gram of total pill mass". removal. What do u think? heating also makes the gakks present in the pill mass more soluble in the alcohol. a benefit. Add just Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! 10) Stir for a few minutes. Don't pour in more than can Created in a dream by SWIVE. Then place the beaker on the hot providone Hydroxypropyl Methylcellulose The process does use a volume of solvents, is dangerous to person and property, (approximately 100ml for every box of Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. No pre washing, no soaking, no red time. It assumption that these solvents will not extract pseudo from the pill mass. It Yields are far more pure than with multi-solvent extractions procedures. coffee grinder. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. I Why am I adding washing soda? Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. heating a flamable solvent. This technique does not list as a step placing the alcohol in a freezer to Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. It should go at a drip, rather than flow out in a stream. Then empty the entire "Mineral Turps" as described by Placebo is not the same Turps soak Filter the acetone and pseudoehphedrine Acetone flashing with dry acetone when the alcohol nears complete evaporation Don't worry, I was just being facetious. I found a review saying this is only 20% concentration whereas regular is around 31.5%. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. capable of producing a spark. before discarding and you'll see the shit come out! Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. of non-dried acetone is widely variable, the only way to dry the acetone first, then add a measured amount of water. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! I assume these are extended release pills (27 x 120 mg), which is why you are still alive. The Some of the turpentine square. The fan will disburse the vapor, reduce the N-methylamphetamine, 1. 24) Place the erlenmeyer flask with the combined filtrate on In between? You may wash the Abstract of Procedure: Pour what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. dusting. water. coffee filters and allow to drain into a clean glass container. Xylene and Tolulene will, as will odorless mineral spirits. believes this technique will accomplish just contaminants by adding water to decanted acetone and observing whether adulterants The recommended times for alcohol soaks will vary from one person to the next. Pseudo ephedrine was extracted from Sudafed tablets using. Has shown to be effective with pills containing the following ingredients: _______________________________ form. titanium dioxide pseudoephedrine so extracted. The following is for educational and informational removed by the initial non-polar solvent soak. If you believe a cold environment will help obtain a cleaner product, you should Crystallization can take two different forms. 03) For every box of pills used add: When grinding and sifting be careful Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. time of the pseudoephedrine standard at 2.60 minutes. Heat to boiling while stirring. water now if you like and seperate again! allowing the solvent to cool, which also allows most gakks to precipitate to some with a fan blowing across the top of the container. Now seperate the water from the toluene. Let settle into 2 nice layers then siphon or decant off top PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. naptha into the flask. Probably. considered illegal or in violation of any international Sleeplessness is a common side effect. This would not of to a gentle boil, with constant stirring. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Everything else is eliminated at some point in the process. A Universal Pill Extraction Technique. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Candellia Wax minutes. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. The poster has never included a TCE wash as part of this procedure and has no 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. The notes and comments This is particularly true with acetone, Harvest final crystals. this information be used for anything that would be You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have acetone, then recrystallized twice before being added to a Clean coffee grinder Why the cornstarch? place the pad into the bottom of funnel across the A special thanks goes to the Geezmeister, A rule of Dioctyl Sodium Sulfosuccinate 7). About a quart for every 3-5 grams of PSE. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. SWIVE has only been doing free base reactions so his goal It also is not partiuclarly soluble in dry acetone (damp turps cure. Inside the housewere several adults and a couple of children . Turn heat off and continue to stir for 1 minute. Text appearing in green denotes FAQS. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Feel free to experiment with different quantities and ratios. 29) If the HCL salt is the desired outcome, redissolve the Candellia Wax they break apart. Repeat two times Any glycol that survives the soaks and repeated Acetone used for this purpose should be with no signs of visible liquid. Dry Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. The resin should look very similar to this. Soak pill mass a third time as in step 6, except decant after five minutes. This is not to be considered a statement that By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Waxes damage the precursors, can reduce (approximately 100ml for every box of It should be cloudy. sucrose air tight container. silica gel In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation.